Micro-Processing
Micro-processing has the unique functionality that it enables
you to produce test-samples from only a few grams of material,
typically 2-15 ml. The advantage of micro-processing over normal
processing is its small scale, resulting in the consumption of
less material (base + additive), reduced processing time and more
and faster data. Therefore micro-processing gives you the opportunity
to generate more data in less time at minimum costs.
Functionally processing consists of 2 steps: 1) compounding or
mixing (in the case of polymers also melting) and 2) shaping. Because
only a few grams of material is consumed in the first step, a fundamental
change in the compounding step was necessary. Normally compounders
are operated in continuous mode, but micro-compounders typically
operate in batch-mode. Residence time is controlled by a 3-way
valve and not by screw geometry like conventional machines. Its
position determines whether compounded material is recirculated,
or guided to the outlet of the compounder. Next to batch-mode,
all micro-compounder are able to process materials in continuous
mode for film and fiber applications The compounders are equipped
with two conical fully intermeshing co rotating screws to ensure
maximum dispersion (exfoliation) or counter rotating screws for
processing shear sensitive materials.
The compounding step means that a base material is mixed with
additives to form a homogeneous mixture. Alternatively, newly synthesized
base material (without additives) can also be compounded in order
to obtain its nascent material properties.
Compounded material is further shaped for testing purposes. There
are many ways to shape. Below you find the most common:
- The simplest way of shaping occurs when compounded material
exits the compounder via a round die. This yields a strand, which
can be further analyzed (e.g. TEM or SEM).
- Another way of shaping your compounded material is to further
process it into a molded certified test-sample by a micro injection
molding machine. The micro injection molding machine can be fed
by our micro compounder – via a preheated transfer cylinder – in
order to obtain standard test bars or any other desired shape,
such as pills, rings, etc without changing their thermal history.
- A 3rd example of shaping takes place when instead of the standard
round die, a slit-die is mounted onto the compounder barrel.
This gives a cast film with typical dimensions between a few
hundred microns down to <5 micron and a typical width of 35
mm. The micro-cast film device is a logical step in our ambition
to broaden the portfolio, the desire to satisfy customers needs
hence a direct consequence of our customer intimacy policy.
- A last example of shaping given here is the production of a
fiber. Typically a mono filament is produced from a few ml of
compounded material. Depending on the diameter of the dye and
the draw-ratio a certain filament thickness is obtained. This
filament can gain even higher draw-ratios in a next step via
thermal stretching, in which the filament is guided through an
oven.
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